Relationship between enamel bond fatigue durability and surface free-energy characteristics with universal adhesives

Yuko Nagura, Akimasa Tsujimoto, Wayne W. Barkmeier, Hidehiko Watanabe, William W. Johnson, Toshiki Takamizawa, Mark A. Latta, Masashi Miyazaki

Research output: Contribution to journalArticle

1 Citation (Scopus)

Abstract

The relationship between enamel bond fatigue durability and surface free-energy characteristics with universal adhesives was investigated. The initial shear bond strengths and shear fatigue strengths of five universal adhesives to enamel were determined with and without phosphoric acid pre-etching. The surface free-energy characteristics of adhesive-treated enamel with and without pre-etching were also determined. The initial shear bond strength and shear fatigue strength of universal adhesive to pre-etched enamel were higher than those to ground enamel. The initial shear bond strength and shear fatigue strength of universal adhesive to pre-etched enamel were material dependent, unlike those to ground enamel. The surface free-energy of the solid (γS) and the hydrogen-bonding force (γSh) of universal adhesive-treated enamel were different depending on the adhesive, regardless of the presence or absence of pre-etching. The bond fatigue durability of universal adhesives was higher to pre-etched enamel than to ground enamel. In addition, the bond fatigue durability to pre-etched enamel was material dependent, unlike that to ground enamel. The surface free-energy characteristics of universal adhesive-treated enamel were influenced by the adhesive type, regardless of the presence or absence of pre-etching. The surface free-energy characteristics of universal adhesive-treated enamel were related to the results of the bond fatigue durability.

Original languageEnglish (US)
Pages (from-to)135-145
Number of pages11
JournalEuropean Journal of Oral Sciences
Volume126
Issue number2
DOIs
StatePublished - Apr 2018

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Dental Enamel
Adhesives
Fatigue
Shear Strength
Hydrogen Bonding

Keywords

  • dental bonding
  • dental debonding
  • dental etching
  • dental restoration failure

ASJC Scopus subject areas

  • Dentistry(all)

Cite this

Relationship between enamel bond fatigue durability and surface free-energy characteristics with universal adhesives. / Nagura, Yuko; Tsujimoto, Akimasa; Barkmeier, Wayne W.; Watanabe, Hidehiko; Johnson, William W.; Takamizawa, Toshiki; Latta, Mark A.; Miyazaki, Masashi.

In: European Journal of Oral Sciences, Vol. 126, No. 2, 04.2018, p. 135-145.

Research output: Contribution to journalArticle

Nagura, Y, Tsujimoto, A, Barkmeier, WW, Watanabe, H, Johnson, WW, Takamizawa, T, Latta, MA & Miyazaki, M 2018, 'Relationship between enamel bond fatigue durability and surface free-energy characteristics with universal adhesives', European Journal of Oral Sciences, vol. 126, no. 2, pp. 135-145. https://doi.org/10.1111/eos.12398
Nagura, Yuko ; Tsujimoto, Akimasa ; Barkmeier, Wayne W. ; Watanabe, Hidehiko ; Johnson, William W. ; Takamizawa, Toshiki ; Latta, Mark A. ; Miyazaki, Masashi. / Relationship between enamel bond fatigue durability and surface free-energy characteristics with universal adhesives. In: European Journal of Oral Sciences. 2018 ; Vol. 126, No. 2. pp. 135-145.
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