N-Acetyl-5-chloro-3-nitro-L-tyrosine ethyl ester

Teresa T. Mutahi, Benson J. Edagwa, Frank R. Fronczek, Rao M. Uppu

Research output: Contribution to journalArticle

Abstract

The title compound, C13H15ClN2O 6, was synthesized by hypochlorous acid-mediated chlorination of N-acetyl-3-nitro-l-tyrosine ethyl ester. The OH group forms an intramolecular O - H⋯O hydrogen bond to the nitro group and the N - H group forms an Intermolecular N - H⋯O hydrogen bonds to an amide O atom, linking the molecules into chains along [100]. The crystal studied was a non-merohedral twin, with a 0.907 (4):0.093 (4) domain ratio.

Original languageEnglish (US)
Pages (from-to)o2810-o2811
JournalActa Crystallographica Section E: Structure Reports Online
Volume68
Issue number9
DOIs
StatePublished - Sep 1 2012

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tyrosine
esters
Esters
Hydrogen bonds
Hypochlorous Acid
Chlorination
Amides
hydrogen bonds
chlorination
Atoms
amides
Crystals
Molecules
Acids
acids
crystals
atoms
nitrotyrosine ethyl ester
molecules
ethyl tyrosine ester

ASJC Scopus subject areas

  • Chemistry(all)
  • Materials Science(all)
  • Condensed Matter Physics

Cite this

N-Acetyl-5-chloro-3-nitro-L-tyrosine ethyl ester. / Mutahi, Teresa T.; Edagwa, Benson J.; Fronczek, Frank R.; Uppu, Rao M.

In: Acta Crystallographica Section E: Structure Reports Online, Vol. 68, No. 9, 01.09.2012, p. o2810-o2811.

Research output: Contribution to journalArticle

Mutahi, Teresa T. ; Edagwa, Benson J. ; Fronczek, Frank R. ; Uppu, Rao M. / N-Acetyl-5-chloro-3-nitro-L-tyrosine ethyl ester. In: Acta Crystallographica Section E: Structure Reports Online. 2012 ; Vol. 68, No. 9. pp. o2810-o2811.
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