Influence of water storage on fatigue strength of self-etch adhesives

Toshiki Takamizawa, Wayne W. Barkmeier, Akimasa Tsujimoto, Donal D. Scheidel, Hidehiko Watanabe, Robert L. Erickson, Mark A. Latta, Masashi Miyazaki

Research output: Contribution to journalArticle

28 Citations (Scopus)

Abstract

Objectives The purpose of this study was to determine enamel and dentin bond durability after long-term water storage using self-etch adhesives. Methods Two single step self-etch adhesives (SU, Scotchbond Universal and GB, G-Ó•nial Bond) and a two-step self-etch adhesive (OX, OptiBond XTR) were used. The shear bond strength (SBS) and shear fatigue strength (FS) of the enamel and dentin were obtained with and without phosphoric acid pre-etching prior to application of the adhesives. The specimens were stored in distilled water at 37 °C for 24 h, 6 months, and one year. A staircase method was used to determine the FS using a frequency of 10 Hz for 50,000 cycles or until failure occurred. Results The SBS and FS of enamel bonds were significantly higher with pre-etching, when compared to no pre-etching for the same water storage period. The FS of dentin bonds with pre-etching tended to decrease relative to no pre-etching at the same storage period. For the one year storage period, SU and GB with pre-etching showed significantly lower FS values than the groups without pre-etching. Conclusions The influence of water storage on FS of the self-etch adhesives was dependent on the adhesive material, storage period and phosphoric acid pre-etching of the bonding site. Clinical significance Phosphoric acid pre-etching of enamel improves the effectiveness of self-etch adhesive systems. Inadvertent contact of phosphoric acid on dentin appears to reduce the ability of self-etch adhesives to effectively bond resin composite materials.

Original languageEnglish (US)
Pages (from-to)1416-1427
Number of pages12
JournalJournal of Dentistry
Volume43
Issue number12
DOIs
StatePublished - Dec 1 2015

Fingerprint

Adhesives
Fatigue
Dentin
Dental Enamel
Water
Shear Strength
Composite Resins
phosphoric acid

Keywords

  • Fatigue strength
  • Long-term water storage
  • Phosphoric acid pre-etching
  • Self-etch adhesive

ASJC Scopus subject areas

  • Dentistry(all)

Cite this

Takamizawa, T., Barkmeier, W. W., Tsujimoto, A., Scheidel, D. D., Watanabe, H., Erickson, R. L., ... Miyazaki, M. (2015). Influence of water storage on fatigue strength of self-etch adhesives. Journal of Dentistry, 43(12), 1416-1427. https://doi.org/10.1016/j.jdent.2015.10.018

Influence of water storage on fatigue strength of self-etch adhesives. / Takamizawa, Toshiki; Barkmeier, Wayne W.; Tsujimoto, Akimasa; Scheidel, Donal D.; Watanabe, Hidehiko; Erickson, Robert L.; Latta, Mark A.; Miyazaki, Masashi.

In: Journal of Dentistry, Vol. 43, No. 12, 01.12.2015, p. 1416-1427.

Research output: Contribution to journalArticle

Takamizawa, T, Barkmeier, WW, Tsujimoto, A, Scheidel, DD, Watanabe, H, Erickson, RL, Latta, MA & Miyazaki, M 2015, 'Influence of water storage on fatigue strength of self-etch adhesives', Journal of Dentistry, vol. 43, no. 12, pp. 1416-1427. https://doi.org/10.1016/j.jdent.2015.10.018
Takamizawa T, Barkmeier WW, Tsujimoto A, Scheidel DD, Watanabe H, Erickson RL et al. Influence of water storage on fatigue strength of self-etch adhesives. Journal of Dentistry. 2015 Dec 1;43(12):1416-1427. https://doi.org/10.1016/j.jdent.2015.10.018
Takamizawa, Toshiki ; Barkmeier, Wayne W. ; Tsujimoto, Akimasa ; Scheidel, Donal D. ; Watanabe, Hidehiko ; Erickson, Robert L. ; Latta, Mark A. ; Miyazaki, Masashi. / Influence of water storage on fatigue strength of self-etch adhesives. In: Journal of Dentistry. 2015 ; Vol. 43, No. 12. pp. 1416-1427.
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abstract = "Objectives The purpose of this study was to determine enamel and dentin bond durability after long-term water storage using self-etch adhesives. Methods Two single step self-etch adhesives (SU, Scotchbond Universal and GB, G-{\'O}•nial Bond) and a two-step self-etch adhesive (OX, OptiBond XTR) were used. The shear bond strength (SBS) and shear fatigue strength (FS) of the enamel and dentin were obtained with and without phosphoric acid pre-etching prior to application of the adhesives. The specimens were stored in distilled water at 37 °C for 24 h, 6 months, and one year. A staircase method was used to determine the FS using a frequency of 10 Hz for 50,000 cycles or until failure occurred. Results The SBS and FS of enamel bonds were significantly higher with pre-etching, when compared to no pre-etching for the same water storage period. The FS of dentin bonds with pre-etching tended to decrease relative to no pre-etching at the same storage period. For the one year storage period, SU and GB with pre-etching showed significantly lower FS values than the groups without pre-etching. Conclusions The influence of water storage on FS of the self-etch adhesives was dependent on the adhesive material, storage period and phosphoric acid pre-etching of the bonding site. Clinical significance Phosphoric acid pre-etching of enamel improves the effectiveness of self-etch adhesive systems. Inadvertent contact of phosphoric acid on dentin appears to reduce the ability of self-etch adhesives to effectively bond resin composite materials.",
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AU - Watanabe, Hidehiko

AU - Erickson, Robert L.

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AU - Miyazaki, Masashi

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N2 - Objectives The purpose of this study was to determine enamel and dentin bond durability after long-term water storage using self-etch adhesives. Methods Two single step self-etch adhesives (SU, Scotchbond Universal and GB, G-Ó•nial Bond) and a two-step self-etch adhesive (OX, OptiBond XTR) were used. The shear bond strength (SBS) and shear fatigue strength (FS) of the enamel and dentin were obtained with and without phosphoric acid pre-etching prior to application of the adhesives. The specimens were stored in distilled water at 37 °C for 24 h, 6 months, and one year. A staircase method was used to determine the FS using a frequency of 10 Hz for 50,000 cycles or until failure occurred. Results The SBS and FS of enamel bonds were significantly higher with pre-etching, when compared to no pre-etching for the same water storage period. The FS of dentin bonds with pre-etching tended to decrease relative to no pre-etching at the same storage period. For the one year storage period, SU and GB with pre-etching showed significantly lower FS values than the groups without pre-etching. Conclusions The influence of water storage on FS of the self-etch adhesives was dependent on the adhesive material, storage period and phosphoric acid pre-etching of the bonding site. Clinical significance Phosphoric acid pre-etching of enamel improves the effectiveness of self-etch adhesive systems. Inadvertent contact of phosphoric acid on dentin appears to reduce the ability of self-etch adhesives to effectively bond resin composite materials.

AB - Objectives The purpose of this study was to determine enamel and dentin bond durability after long-term water storage using self-etch adhesives. Methods Two single step self-etch adhesives (SU, Scotchbond Universal and GB, G-Ó•nial Bond) and a two-step self-etch adhesive (OX, OptiBond XTR) were used. The shear bond strength (SBS) and shear fatigue strength (FS) of the enamel and dentin were obtained with and without phosphoric acid pre-etching prior to application of the adhesives. The specimens were stored in distilled water at 37 °C for 24 h, 6 months, and one year. A staircase method was used to determine the FS using a frequency of 10 Hz for 50,000 cycles or until failure occurred. Results The SBS and FS of enamel bonds were significantly higher with pre-etching, when compared to no pre-etching for the same water storage period. The FS of dentin bonds with pre-etching tended to decrease relative to no pre-etching at the same storage period. For the one year storage period, SU and GB with pre-etching showed significantly lower FS values than the groups without pre-etching. Conclusions The influence of water storage on FS of the self-etch adhesives was dependent on the adhesive material, storage period and phosphoric acid pre-etching of the bonding site. Clinical significance Phosphoric acid pre-etching of enamel improves the effectiveness of self-etch adhesive systems. Inadvertent contact of phosphoric acid on dentin appears to reduce the ability of self-etch adhesives to effectively bond resin composite materials.

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