Determination of vanadium in biological tissue by anion exchange chromatography and neutron activation analysis

A. J. Blotcky, Frederick G Hamel, A. Stranik, A. Ebrahim, R. B. Sharma, E. P. Rack, S. S. Solomon

Research output: Contribution to journalArticle

4 Citations (Scopus)

Abstract

A method is described for determination of vanadium in biological tissues. This method consists of a wet digestion of the tissue with nitric acid followed by anion exchange chromatography, neutron irradiation, and radioassay. The chromatographic separation will allow the decontamination of vanadium from radioactivatable sodium and chlorine which are present in large quantities in biological tissues. The validity of the method is evaluated by employing NBS-SRM 157 and 157a Bovine Liver employing the method of standard additions. The method is successfully applied to human, cow and rat liver specimens. The detection limit of the method is one ppb.

Original languageEnglish (US)
Pages (from-to)319-329
Number of pages11
JournalJournal of Radioanalytical and Nuclear Chemistry Articles
Volume131
Issue number2
DOIs
StatePublished - Jun 1 1989

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Neutron Activation Analysis
Vanadium
Neutron activation analysis
Chromatography
Anions
Ion exchange
Negative ions
Tissue
Liver
Nitric Acid
Decontamination
Neutron irradiation
Chlorine
Nitric acid
Rats
Sodium
Neutrons
Limit of Detection
Digestion

ASJC Scopus subject areas

  • Analytical Chemistry
  • Nuclear Energy and Engineering
  • Radiology Nuclear Medicine and imaging
  • Pollution
  • Spectroscopy
  • Public Health, Environmental and Occupational Health
  • Health, Toxicology and Mutagenesis

Cite this

Determination of vanadium in biological tissue by anion exchange chromatography and neutron activation analysis. / Blotcky, A. J.; Hamel, Frederick G; Stranik, A.; Ebrahim, A.; Sharma, R. B.; Rack, E. P.; Solomon, S. S.

In: Journal of Radioanalytical and Nuclear Chemistry Articles, Vol. 131, No. 2, 01.06.1989, p. 319-329.

Research output: Contribution to journalArticle

Blotcky, A. J. ; Hamel, Frederick G ; Stranik, A. ; Ebrahim, A. ; Sharma, R. B. ; Rack, E. P. ; Solomon, S. S. / Determination of vanadium in biological tissue by anion exchange chromatography and neutron activation analysis. In: Journal of Radioanalytical and Nuclear Chemistry Articles. 1989 ; Vol. 131, No. 2. pp. 319-329.
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